Category: Barbara

Thursday, 9 May 2013

09:49 – Barbara just left for the hospital. They’re discharging her dad this morning and transporting him to the Brian Center nursing/rehab facility. It’s one of the best ones available, and it’s where my mom lived for a year before her final illness. It’s also only about a mile from our house, which’ll make it a lot easier for Barbara to visit. Barbara’s sister works not far from it, so it’ll be easy for her to visit as well. No word yet on when Sankie will be released, but it may be this weekend. She’s recovering well, emotionally as well as physically, and told Barbara she wants to go back to their apartment at Creekside Retirement Village. Once she’s off the IV antibiotics, I’m sure they’ll be taking her home.

I was getting low on pipe tobacco, so I ordered five pounds (2.3 kilos) yesterday. It’s a Dunhill My Mixture 965 clone, and it cost me about $27/pound, with free shipping. Years ago, I used to smoke the real Dunhill 965, but Dunhill hasn’t actually produced it for many years. Instead, they license out the name. They’ve done that serially with two or three different manufacturers over the years, and it’s never been the same as the original stuff. The clone I ordered is actually better than the branded stuff from the current manufacturer, which costs about twice as much as the clone. The vendor was backordered for a couple weeks on the clone 965 product, which is fine. I always reorder when I get down to my last pound, and five pounds lasts me about seven months.

While I was on the phone with the vendor, I asked the guy about the possible new taxes on pipe tobacco. He said they were following the matter, but had no real idea if or when these new taxes would come into play. I’ve heard numbers as high as $100/pound in new taxes, and told the guy they needed to keep their mailing list updated on when these new taxes would come into effect so that we could stock up before the price skyrocketed. I also told him that I was in North Carolina and if it really came to that I’d just start growing my own.

Since I was making phone calls anyway, I decided to call DMV to make an appointment to renew my driver’s license, which expires next month. After getting busy signals several times, I finally got through and told the guy that answered that I wanted to make an appointment. He said “just a moment” and put me on hold. Eighteen minutes later, the call disconnected. So I called back, getting busy signals several times, and finally got a person on the line. I told him I’d been dropped after 18 minutes on hold. He apologized and … put me on hold. Fortunately, this time someone picked up after about 15 seconds and made the appointment for me.

I was on a roll, so I decided to call Time-Warner Cable tech support and see if they could do something about the Internet problems we’d been having for several days. They’d gotten much worse by yesterday, and I ended up connected to a nice young woman, who said that my modem had been up for six months and needed to be reset. She verified that we had Internet service and basic cable TV. She said the modem was a TWC Internet + VoIP modem. I explained that we formerly had VoIP but no longer had it. She said, “So you’re talking to me on a phone?” I said, “Yes, but …” She said “I’ll reset your modem now.” I continued “we’re on a third-party VoIP service so if you reset the modem you’ll kill our call”, but I was talking to dead air. I looked down to see the modem lights resetting. Oh, well. The reset worked, and our Internet is now running normally.

I managed to get 30 sets of the LK01 Life Science chemical bags made up yesterday, and 30 sets of the small parts bags. Today I’ll assemble shipping boxes for them and get some finished kits built. Then I’d better start on a new batch of biology kits, because we’re down to 20 or so of those in stock.


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Wednesday, 8 May 2013

09:13 – We’re in reasonably good shape with regard to finished-goods inventory on our current science kits, with 70 or 80 assorted ones in stock. Over the next couple days, I’ll make up 30 sets of chemical bags and small parts bags for the LK01 Life Science kits. This weekend we’ll build the shipping boxes and assemble 30 LK01 kits to be ready to start shipping them Monday.

With both parents still in the hospital, Barbara and Frances are still waiting to find out when they’ll be discharged, and where they’ll be discharged to. It’s pretty clear that Dutch will have to be discharged to a nursing home, but there’s no way to know which one because it all depends on which nursing homes have a bed available at the time he’s discharged. We’re hoping that Sankie will be well enough to return to their apartment at Creekside, but we won’t know that for sure until she’s ready to be discharged.


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Tuesday, 7 May 2013

08:11 – With Barbara’s mom and dad both in the hospital, she and Frances are even busier than usual. They expect Dutch to be discharged late this week, and are looking at assisted-living facilities to decide which are acceptable to have Dutch transferred to. Their mom is being treated for a lung infection, and they’re not sure at this point how long she’ll be in the hospital or whether she’ll be going home to the apartment or will need to go to an assisted-living facility for at least a while. We’re hoping that Sankie’s outlook will improve sufficiently that she’ll be able to return directly to their apartment.

I’m busy putting together subassemblies for a first batch of thirty LK01 Life Science Kits. At this point, it’s all a matter of assembly except that we’re out of stock on bottles of methyl cellulose. I have two liters of that made up, but none bottled. The second bottle-top dispenser I ordered arrived yesterday, so I just need to get some bottles filled. We announced that the LK01 kits would begin shipping the week of 26 May, but we may in fact have them ready to start shipping as early as next Monday.


11:00 – One thing I didn’t think about when we decided to start building and selling science kits is the amount of physical labor involved, particularly as our sales ramp up. I just hauled four cases of goggles downstairs and stacked them. On the return trips upstairs, I’m hauling up finished kits, five at a time. I have about four dozen kits to haul up and more stuff to haul down. And UPS should show up today with a couple cases of 144 glass beakers and several cases of 100 mL graduated cylinders. If I catch Don as he pulls up, I’ll ask him to roll those crates around back to save me having to carry them downstairs.

I tend to think of components as small, light items, which is true individually. How much can a stainless-steel spatula or a glass stirring rod weigh, after all? But put a case of 700 of each of them in a large box along with similar quantities of two or three other “small, light” items, and the mass adds up quickly. At 30, I wouldn’t have thought twice about any of this stuff; at nearly 60, it becomes an aerobic workout. Between hauling components and kits up and down the stairs and walking Colin, I probably get more exercise than most guys my age.


14:56 – Urk. Now that’s embarrassing. I’m starting to clean off my main desk to make room for the new system. I’m going to run it side-by-side with the current system until I’m sure everything I need is migrated over. So, as I was moving piles of stuff off my desk, what did I notice but a stack of five hard drives in those clear plastic form-fitted cases. I looked at the first one: “Oh, well, it’s only 160 GB, not big enough to worry about.” At the second: “Oh, well, it’s only 500 GB.” At the third: “Oh, well, it’s only 1.5 TB.” At the fourth: “Oh, well, it’s only, uh, 2 TB.” At the fifth: “Oh, shit. Another 2 TB drive.” Both 2 TB drives, as best I remember, have never been used other than briefly to test a RAID system. Oh, well. One can never have too many hard drives. I’d completely forgotten I had these. I’ll probably just stick them in an external eSATA drive carrier and use them for portable backup.


16:20 – With Europe already turning into a smoking pile of rubble, I sometimes wonder if Comrade Barroso has been inhaling too much of that smoke: Federal Europe will be ‘a reality in a few years’, says Jose Manuel Barroso

Federated, hell. They’ll be lucky if the EU still exists. The euro certainly won’t, unless it’s a Southern-tier euro, with the protestant Northern tier returning to their own currencies, or perhaps, if they haven’t learned their lesson from this catastrophe, a shared Deutsche Mark under whatever name. I’ve known for years that Barroso, that “former” Marxist, is delusional, but he keeps coming up with even more impressive castles in the sky. Barroso, who defines the term True Believer, no doubt actually believes that not just the eurozone but the EU 27 will fall in with his ridiculous plans. Even now, the UK is teetering on the edge of withdrawing from the EU, and with prominent defections among even his own Tories, Cameron may not be able to hold things together for another year, let alone until the proposed referendum on EU membership four years from now. And what are the chances that Germany, Finland, and Holland will agree to pay not just the Southern tier’s outstanding debts but to continue to subsidize them forever and without limit? I’d say the probability is slightly more than zero. Maybe 0.000001.

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Monday, 6 May 2013

09:20 – Barbara’s dad is doing better, but it’s looking like he’ll never be able to live at the retirement village apartment. It’s “independent living”, and at this point Dutch needs at least “assisted living”, if not yet a nursing home. Barbara and Frances are looking at options. Apparently, the hospital has provided them with a list of such facilities so that they can review them. When it comes time to discharge Dutch, the hospital will give them a subset of that list–the ones that have beds available–and then discharge Dutch directly to the family’s choice of facility. Although assisted-living facilities are more expensive than independent-living ones, Barbara’s parents’ actual out-of-pocket expenses may not change much, if at all. Dutch’s VA insurance doesn’t pay anything toward their current costs because they’re in independent living; if he or he and Sankie move to an assisted-living facility, the VA insurance starts paying part of the costs.

Meanwhile, Sankie is starting to break down physically under the stress. Basically, she knows that she can’t take care of Dutch in their apartment, and she’s not even comfortable with being there by herself. She’s exhausted and stressed out. What she really wants is Barbara and/or Frances to be there with her 24 hours a day, which obviously isn’t going to happen. Sankie does have long-term care insurance that will pay if she’s in an assisted-living facility or nursing home, so the best solution may be to find an assisted-living facility that will accept both Dutch and Sankie and allow them to share a room. The downside is that most such facilities have small rooms, so they wouldn’t be able to take many of their possessions along with them. Still, the combination of having round-the-clock help available on-site and being able to continue living together may be enough to make that the best option. The other option is to move Dutch to assisted-living and leave Sankie where she is. Of course, with that option, she’s not going to have someone with her constantly. Until a week or so ago, Sankie seemed content with the idea of living at Creekside by herself after Dutch dies. Now she’s worried that she won’t be able to make it on her own, but we’re hoping that’s only because she’s exhausted and possibly ill at the moment. We’re hoping that things work out as well as possible for Dutch and Sankie, which would also take a great deal of the stress off of Barbara and Frances.


11:58 – I haven’t said much about this new initiative to force businesses to collect and remit sales taxes on interstate sales because I’ve been waiting to see what happens. The bill appears to be likely to pass the Senate, although it may founder in the House. I hope so.

The problem with this bill is that it violates the Constitution on its face. States are not permitted to interfere with interstate commerce. North Carolina, for example, cannot set up a customs station at the Virginia border and impose an import duty on goods crossing into North Carolina. Nor can North Carolina tax a transaction that does not occur fully within North Carolina. If I sell a kit to a buyer in another state, neither state can Constitutionally tax that transaction, because it did not occur fully within either state. Attempting to tax that transaction is interfering with interstate commerce, which the Constitution prohibits states from doing.

In fact, the whole “nexus” idea violates the Constitution. If I visit the local Wal*Mart and purchase an item, Wal*Mart can legally collect sales tax from me. But if I visit Wal*Mart.com and purchase an item, the fact that Wal*Mart has physical stores in North Carolina is insufficient for North Carolina to tax that sale. That sale did not occur fully within North Carolina, so in taxing it North Carolina is interfering with interstate commerce, thereby violating the Constitution.

The same holds true for so-called “use taxes”, which are transparent attempts to enforce extraterritoriality, again in violation of the Constitution. If I buy an item from Amazon, the Constitution prohibits North Carolina from charging a sales tax. Calling it a “use tax” doesn’t make it allowable, unless North Carolina also charges that use tax on local purchases, in addition to the sales tax. And, of course, forcing any business to collect sales taxes (or any other type of taxes) on the governments’ behalf is prohibited Constitutionally, if nothing else by the amendment that prohibits involuntary servitude.

The only minor concession this proposed new law makes is to exempt small business with revenues under $1,000,000 annually from collecting sales taxes for roughly 9,000 separate tax jurisdictions. So, our way forward is clear. We will simply refuse to allow our revenues to exceed $1 million annually. If we eventually get to the point where $1 million in annual revenues is a real possibility, we’ll simply incorporate a second, legally separate business and split the sales between the two businesses.


13:46 – Barbara called a little while ago to say that her sister was taking their mom to the hospital. Frances had taken Sankie to a doctor’s appointment, and apparently the doctor thought she should be in the hospital. Sankie has suffered for years from recurring lung problems, and she apparently has some kind of lung infection again. The doctor talked about possibly sending her home with a prescription for azithromycin, but when Frances explained that there was no one to stay with her mom around the clock, he apparently decided to admit her to the hospital and put her on stronger antibiotics. Barbara and Frances suspected she might have another lung infection and that that was causing or at least contributing to her problems over the last few days. We hope they’ll get Sankie cured and back to her apartment soon. So now Barbara and Frances have not one but both parents in the hospital, and in not one but two different hospitals. Geez.

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Sunday, 5 May 2013

07:55 – Barbara left yesterday morning to run some errands and then head over to her parents’ apartment to pick up a few items for her dad before visiting him in the hospital. While she was gone, I got a call from a young woman at the hospital, whom I assumed to be one of the nurses caring for Dutch. She was calling to give Barbara an update on her dad’s condition, so I gave her Barbara’s cell phone number. She said I wasn’t on Dutch’s HIPAA list, so she wasn’t allowed to tell me anything, but asked since she already had me on the phone if I’d mind her asking a few questions about Dutch. I answered as best I could based on what Barbara has been telling me. She thanked me before she hung up. It wasn’t until I talked to Barbara later that I found out she wasn’t a nurse. She was one of Dutch’s doctors. At first, I wondered if I’d been unconsciously sexist/agist, but that wasn’t it at all. I assumed that she was a nurse because she wasn’t at all hurried or arrogant. She took her time and didn’t seem to be at all in a hurry to finish the conversation and move on to the next item on her to-do list. She talked to me as though I were an intelligent person who might have useful information rather than just someone she had to talk to to complete a checklist. I suspect that Dutch is lucky to be her patient.

The replacement hard drive for my new system arrived several days ago, but I hadn’t had a spare moment to do anything with it. While Barbara was away yesterday afternoon, I took the time to install the drive and get Linux Mint 13 LTS up and running. The system is still sitting on the kitchen table, but it’ll shortly move into my office, where it will sit, along with its new monitor, keyboard, and mouse, alongside my current system. I’ll run them side-by-side until I’m satisfied that everything I care about on the current system–apps and data and configurations–has been migrated successfully to the new system. Then and only then I’ll do a cut-over.

I’d originally planned to install the system to the 128 GB SSD, but I changed my mind. I installed Linux to the hard drive, and will use the SSD as a second drive devoted exclusively to data. When I leave the house for anything more than walking Colin, I’ll unmount the SSD, slide it out of its bay, and take it along.


09:33 – I just boxed up another forensic science kit and set it out to ship tomorrow. That’s the third one in the last week, which is about two more than I’d expect to sell in a week this time of year. (The biology kits and chemistry kits both ordinarily outsell the forensic science kits by a factor of four or five.) We’re down to only six forensic science kits in stock, so we’d better get another 30 built soon. Or at least get the small parts bags made up and the chemicals bottled and bagged. Given those, we can build kits as needed on the fly.

Going through the list of chemicals and reagents we’ll need for the new batch of forensic kits I noticed glycerol, which is one of my least favorite chemicals to fill bottles with. The stuff is viscous, which makes it very difficult to fill bottles manually because it wants to form a bubble at the bottle’s mouth and then blurp over and run down the side of the bottle. Using the automatic dispenser is easier, but the viscosity of glycerol makes it almost a gym workout to use the pump. Then I realized that the viscosity of glycerol is strongly affected by temperature. At room temperature, the stuff is gloppy. At around body temperature (37 C) to hot tap water temperature (50 C), the stuff is much, much less viscous. So, the next time I fill glycerol bottles, I’m going to run a bucket of hot tap water and put the 3.8 liter stock bottle of glycerol in it to warm up before I dispense it.

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Saturday, 4 May 2013

08:40 – Barbara’s father is back in the hospital. She made a quick stop at the supermarket and library on the way home from work yesterday, and then headed out to cut the grass while I made dinner, timed for 6:30. Around 6:15, Frances called to say that their dad had fallen while getting out of her car on their way back from a doctor’s appointment for their mom. He wasn’t injured, he’d pretty much just sat down rather than actually fallen, but he wasn’t strong enough to get up. Frances got a couple of the staff at their retirement village to help get him up and into his wheelchair. Frances said it wasn’t an emergency, and just to let Barbara know to call her when she finished mowing the lawn. She said they couldn’t leave Dutch with just Sankie to help him, so they were going to have to start staying over there at night.

As I was talking to Frances, my call-waiting beeped, but by the time I was able to hookflash over to the new call it had been disconnected. The caller ID showed it was Barbara’s parents’ apartment calling, so I called back. Sankie answered the phone, obviously very upset. I asked if she’d just called, and she said she had. She said Dutch had fallen and Barbara needed to come over right away to help them. I asked Sankie if she meant that Dutch had fallen again, in the apartment, or if she was talking about his fall out in the parking lot that Frances had just told me about. She was obviously confused, and just hung up. So I called Frances’s cell phone back. She’d been out in the parking lot moving the car, and arrived back in Dutch and Sankie’s apartment just as I called. She said her mom was talking about the fall she’d just told me about, and that he hadn’t fallen again.

I heard Barbara just finishing up outside. When she came upstairs, I told her what was going on. She called Frances back and told her to call 911 and have Dutch transported to the hospital. Barbara said Dutch’s symptoms were exactly what they’d been the last time they’d brought him home from the hospital and had to turn around immediately and take him back. She told Frances that she was going to change clothes, eat a quick dinner, and then head over to the hospital.

Barbara left around 7:00 for the hospital, and got home about 2:30 this morning. I’m sure she’ll post more details on her page when she has time to do so.


10:24 – I’m still trying to get a reasonable projection of what our science kit sales might be for the year. A big part of the problem is that our sales are extremely seasonal. More than 90% of our sales last year occurred in the last seven months of the year. Put it this way, in 2012 we had higher sales in our biggest month (August) than in the first six months of the year combined. And in every month so far in 2013, we’ve had higher revenue in that month than we had in the entire first quarter of 2012.

The scary part is that in 2012 we shipped less than a dozen kits on our biggest day. If the current sales trajectory holds up, in 2013 we may need to be prepared to ship 60 or more kits on a big day, which obviously means we’ll need to have a boatload of kits in inventory come July. I’m not even entirely sure that I can process 60 orders and ship 60 kits in one day. And, of course, the other scary part is what happens if somehow this sales increase is just a blip. I’d hate to end up with several hundred kits in inventory and no orders to fill.

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Wednesday, 1 May 2013

08:22 – Barbara took her dad to the doctor yesterday morning for a follow-up appointment. We didn’t get any phone calls overnight, so apparently Dutch settled in successfully for his first night at home. Barbara is leaving work early this afternoon to take her mother to a doctor’s appointment. Her mom has yet another appointment tomorrow, but Frances is taking her to that one.

We’re now up to about five dozen assorted biology and chemistry kits in finished-goods inventory. I’m building a batch of forensic kits today, using the finished subassemblies we have in stock. Next on the schedule is a batch of 30 life science kits, followed by 60 more biology kits and 60 more chemistry kits. After that, it’ll be lather, rinse, repeat for the rest of this year. May is historically a pretty slow month, about like April. But things start to pick up in June, before the crazy time starts in July and August. June should be about three times the May’s volume, and July and August each three or four times June’s volume. So, for the next six months or so, my life will be spent making up chemicals, filling bottles, issuing purchase orders, building subassemblies and kits, and processing orders and shipping kits. Not that I mind. I like to stay busy, and I like making stuff.


14:28 – I just called Katie Dugan, my vendor rep at American Educational Products, to check price and availability on some items for a purchase order I’m putting together. Every January, AMEP offers four coupons for things like free shipping on any order over $750, a 10% discount on any order over $300, and so on. So, intending to use one of the free shipping coupons, I gave Katie the item numbers and quantities to verify: 30 dozen each 10 mL graduated cylinders and 100 mL graduated cylinders, 30 dozen 250 mL glass beakers, and so on.

I’d also intended to order some chemicals from Katie, mostly the same ones I’d ordered from her late last year. Stuff like 2.5 liters of 30% ammonia, several 500 mL bottles each of n-butanol and glacial acetic acid, and so on. AMEP doesn’t actually carry chemicals, but their sister company, eNasco, does. And the last time I ordered chemicals from Katie, they were actually shipped from eNasco. The problem is, eNasco is retail-oriented, and they apparently have no one on staff who has any clue about hazardous shipping regulations. So for my prior order, eNasco had essentially shipped everything as hazardous, with each bottle as a separate shipment. That means they had to pay a separate hazardous shipping fee for each bottle. What they should have done was combine all of the bottles in one box. If they’d done that, they’d have had to pay only one hazardous shipping surcharge instead of a dozen or more. Needless to say, eNasco billed AMEP for the shipping charges, which probably totaled several hundred dollars rather than the $27 it should have cost them. I apologized to Katie and told her that I’d never have ordered from them if I’d realized how much “free” shipping was going to end up costing them. And I suggested that eNasco really, really needs someone on staff who understands at least the basics of hazardous shipping regulations. That’s non-trivial. In fact, it’s almost a full-time job. Different requirements apply to different chemicals. For example, for shipping under the Limited Quantity Exemption (which is completely different from the Small Quantity Exemption, which in turn is completely different from the ORM-D exemption, which is being eliminated anyway), you may be able to put 5 liters of one chemical in a single package, but only 500 mL of a different chemical. There are also restrictions on which combinations of chemicals are allowed to share a box. As Katie said, they learned an expensive lesson.

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Tuesday, 30 April 2013

09:15 – Barbara called last night around 7:30 to say her dad was back at home and doing pretty well. I was mistaken about Frances staying with their mom and dad tonight. Barbara said they’re going to leave their parents alone tonight and just keep their fingers crossed that Dutch will settle in.

I got another batch of biology kits assembled yesterday. Today, among other things, I’ll start building another batch of two dozen chemistry kits. With what’s already on hand, that should give us enough biology and chemistry kits to last through the end of May. Then I’ll get started on building subassemblies for the first batch of 30 life science kits, which start shipping the last week of May.


13:05 – I thought of Barbara’s father when I saw this:

I’ve assembled four dozen science kits in the last two days, which got me down to dangerously low inventory levels on several items. For example, I’m down to only four 12″ lab thermometers and less than 70 splash goggles. Fortunately, I’d just issued a purchase order this morning for 400 thermometers and 400 splash goggles, along with a bunch of other stuff. That vendor had everything I really needed in stock and they generally ship pretty quickly, so I suspect the stuff will arrive late this week or early next. I was also going to order a couple or three gross of 250 mL glass beakers, but this particular vendor doesn’t stock glassware and sells it only by the case. The trouble is, their lead time on glassware is 90 days give or take. Oh, well. I can get those beakers quickly from any of several other wholesalers.

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Monday, 29 April 2013

10:16 – Barbara’s dad gets his last IV antibiotic dose at 4:00 this afternoon. Barbara and Frances are leaving work early to pick him up from the nursing home and take him back to his apartment at Creekside. Barbara will stay with him tonight because she’s concerned that her mom won’t be able to deal with Dutch physically on her own quite yet. Dutch is now able to stand and walk, but still has some trouble getting up out of a chair and so on. Frances will have dad-sitting duty tomorrow night and then she and Barbara will decide if Dutch is able to be on his own with just Sankie there to help him.

Our finished goods inventory of science kits is getting low again, so I’ll spend some time today and tomorrow assembling more finished kits.


11:52 – Never, ever even think of ordering anything from Vitality Medical. I ordered 500 oral syringes from them a year or so ago, and they’ve been spamming me ever since. At first, it was one or two spams a week. Now it’s up to at least one a day. I’ve repeatedly clicked on the unsubscribe link in their emails, with no effect. I’ve emailed their customer support repeatedly, again with no effect. I’ve called the support number repeatedly, again with no effect.

Yesterday, I finally checked the email headers and found that apparently Vitality Medical subcontracts their spamming out to a company called Constant Contact. No shit. They do what their name says. The FTC needs to shut these bastards down.

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Saturday, 27 April 2013

08:16 – Barbara’s dad’s IV antibiotic course finishes tomorrow. She has to take him to a follow-up visit to his doctor Tuesday, so she’s going to pick him up from the rehab facility and take him back to his apartment after he visits the doctor. She says he’s up and about, which is all that’s necessary to make his own apartment the best place for him. The last thing Barbara and Frances want to do is split up their mom and dad, so they intend to keep him at the Creekside retirement village as long as possible. If/when there’s another crisis, they’ll get him to the hospital and wait until he’s well enough to come straight back home. They don’t want him in a nursing home until/if it’s completely unavoidable.

The heat sealer I ordered from Amazon arrived yesterday, and I immediately put it to the test by sealing a couple of bottles of iodine solution in a quart ziplock bag. The bags are 2-mil (0.05+ mm) polyethylene, and it takes only a couple seconds for the sealer to melt a seal into the bag. I intentionally left plenty of air in the bags so that I could check them for airtightness. They are in fact airtight, but unfortunately that doesn’t stop the iodine vapor from penetrating the bag. There’s a very, very slight iodine odor, but that’s good enough to keep the iodine vapor from staining other parts in the kits. We’re going to start including a separate iodine bottle label that people can affix to the bottle once they open the bag. I’ll probably also use the heat sealer to seal the other chemical bags in the kits.


11:36 – Barbara and I just got back from Lowe’s. We needed some 4-foot fluorescent tubes for the basement fixtures, so we picked up a 10-pack for $22. I think I’ll date the things with a Sharpie before I install them. I think some of the current tubes are original from when we installed the fixtures back in the late 80’s and early 90’s.

While we out there, I decided to pick up some chemicals for the kits. Most of the chemicals we use are reagent-grade, lab-grade, or USP, purchased from lab chemical vendors. But three of them we get from Lowe’s or Home Depot, because we use them in relatively large amounts and they’re much cheaper at a DIY super-center than they are from lab vendors. The purity is adequate for our purposes. Those three are copper(II) sulfate pentahydrate (sold as Root Kill), sodium hydroxide (sold as Crystal Drain Opener), and hydrochloric acid (sold as muriatic acid).

Years ago, before I decided to use them, I did gravimetric analyses on the copper(II) sulfate and sodium hydroxide. The Root Kill ($13 for two pounds/907 grams) is labeled as 99% copper(II) sulfate. When I tested it gravimetrically, it assayed at, IIRC, 99.7±0.1%, which is essentially reagent-grade in terms of purity. The remaining 0.3% give or take is probably almost all insoluble copper(II) oxide, which is easy to filter out. The Crystal Drain Opener is labeled as 100.0% sodium hydroxide. Gravimetrically, I got about 99.5% sodium hydroxide, but I suspect it really is 100.0% in the bottle. The problem with sodium hydroxide is that it literally sucks water vapor out of the air. You can put some dry sodium hydroxide in a weigh boat and watch the weight increase as the dry crystals absorb water. The muriatic acid is probably about lab grade in terms of purity. The stuff is manufactured simply by bubbling hydrogen chloride gas into water, so most of the contaminants in the products were in the source water. Still, it’s more than good enough for our purposes.

I also picked up a gallon (3.8 liters) of acetone in the paint department for something like $4.50 a liter. It’s certainly not spectroscopic-grade nor even reagent-grade acetone, but again it’s more than pure enough for our purposes. Acetone is produced commercially mostly directly from propylene by the cumene process or by oxidizing isopropanol, so the process itself inherently produces pretty pure product. Other than water, the only contaminants are typically low concentrations of VOCs that have no effect on the acetone for solvent purposes. We use it 50/50 with USP-grade 70% IPA for making up Sudan III stain. I’ve tested that stain made up with reagent-grade solvents, and there’s no visible difference in results compared to stain made up with the USP and technical-grade solvents.

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